Method I
1 Scope
This method specifies the sample preparation and high performance liquid chromatography determination method for residue detection of quinolone drugs in milk.
This method is applicable to the single or multi-residue detection of drugs such as ciprofloxacin, danofloxacin, enrofloxacin, sarafloxacin and difloxacin in milk.
2 Normative References
The following referenced document is indispensable for the application of this document. For dated reference, only the edition cited applies. For undated references, the latest edition of the referenced document (including any amendments) applies.
GB/T 6682 Water for Analytical Laboratory Use - Specification and Test Methods
1 Scope
2 Normative References
3 Theory
4 Reagents and Materials
5 Apparatuses
6 Preparation and Preservation of Test Portion
7 Determination Procedures
8 Result Calculation and Expression
9 Sensitivity, Accuracy and Precision of Detection Method
10 Scope
11 Normative References
12 Theory
13 Reagents and Materials
14 Apparatuses
15 Specimen Preparation and Preservation
16 Determination Procedures
17 Result Calculation and Expression
18 Sensitivity, Accuracy and Precision of Detection Method
Annex A Chromatograms
Annex B Chromatograms
Method I
1 Scope
This method specifies the sample preparation and high performance liquid chromatography determination method for residue detection of quinolone drugs in milk.
This method is applicable to the single or multi-residue detection of drugs such as ciprofloxacin, danofloxacin, enrofloxacin, sarafloxacin and difloxacin in milk.
2 Normative References
The following referenced document is indispensable for the application of this document. For dated reference, only the edition cited applies. For undated references, the latest edition of the referenced document (including any amendments) applies.
GB/T 6682 Water for Analytical Laboratory Use - Specification and Test Methods
Contents of GB 29692-2013
1 Scope
2 Normative References
3 Theory
4 Reagents and Materials
5 Apparatuses
6 Preparation and Preservation of Test Portion
7 Determination Procedures
8 Result Calculation and Expression
9 Sensitivity, Accuracy and Precision of Detection Method
10 Scope
11 Normative References
12 Theory
13 Reagents and Materials
14 Apparatuses
15 Specimen Preparation and Preservation
16 Determination Procedures
17 Result Calculation and Expression
18 Sensitivity, Accuracy and Precision of Detection Method
Annex A Chromatograms
Annex B Chromatograms
