GB/T 11064.11-2013 Methods for Chemical Analysis of Lithium Carbonate, Lithium Hydroxide Monohydrate and Lithium Chloride - Part 11: Determination of Acid-insolubles Content - Gravimetric Method (English Version)
Methods for Chemical Analysis of Lithium Carbonate, Lithium Hydroxide Monohydrate and Lithium Chloride - Part 11: Determination of Acid-insolubles Content - Gravimetric Method
1 Scope
This part of GB/T 11064 specifies the methods for determining the acid-insolubles content in the lithium carbonate, lithium hydroxide monohydrate and lithium chloride.
This part is applicable to the determination of acid-insolubles content in the lithium carbonate, lithium hydroxide monohydrate and lithium chloride, within the range of 0.0050%~0.020%.
2 Method summary
The test sample is decomposed with hydrochloric acid, heated and boiled, filtered with a glass filter crucible, and dried at 105%~110% to a constant mass.
3 Reagents
Unless otherwise specified, analytically-pure reagents and distilled or deionized water shall be used for purpose of this part.
3.1 Hydrochloric acid (ρ=1.19 g/mL).
3.2 Methyl orange indicator solution (1 g/L): weigh 0.1g methyl orange, dissolve in 70% of water, cool it and dilute it to 100 mL.
Foreword i
1 Scope
2 Method summary
3 Reagents
4 Apparatus
5 Test sample
6 Analysis procedures
7 Calculation of analysis result
8 Precision
9 Test report
Standard
GB/T 11064.11-2013 Methods for Chemical Analysis of Lithium Carbonate, Lithium Hydroxide Monohydrate and Lithium Chloride - Part 11: Determination of Acid-insolubles Content - Gravimetric Method (English Version)
Standard No.
GB/T 11064.11-2013
Status
valid
Language
English
File Format
PDF
Word Count
4000 words
Price(USD)
80.0
Implemented on
2014-8-1
Delivery
via email in 1 business day
Detail of GB/T 11064.11-2013
Standard No.
GB/T 11064.11-2013
English Name
Methods for Chemical Analysis of Lithium Carbonate, Lithium Hydroxide Monohydrate and Lithium Chloride - Part 11: Determination of Acid-insolubles Content - Gravimetric Method
1 Scope
This part of GB/T 11064 specifies the methods for determining the acid-insolubles content in the lithium carbonate, lithium hydroxide monohydrate and lithium chloride.
This part is applicable to the determination of acid-insolubles content in the lithium carbonate, lithium hydroxide monohydrate and lithium chloride, within the range of 0.0050%~0.020%.
2 Method summary
The test sample is decomposed with hydrochloric acid, heated and boiled, filtered with a glass filter crucible, and dried at 105%~110% to a constant mass.
3 Reagents
Unless otherwise specified, analytically-pure reagents and distilled or deionized water shall be used for purpose of this part.
3.1 Hydrochloric acid (ρ=1.19 g/mL).
3.2 Methyl orange indicator solution (1 g/L): weigh 0.1g methyl orange, dissolve in 70% of water, cool it and dilute it to 100 mL.
Contents of GB/T 11064.11-2013
Foreword i
1 Scope
2 Method summary
3 Reagents
4 Apparatus
5 Test sample
6 Analysis procedures
7 Calculation of analysis result
8 Precision
9 Test report