GB/T 39560.10-2024 Determination of certain substances in electrical and electronic products—Part 10:Polycyclic aromatic hydrocarbons (PAHs) in polymers and electronics by gas chromatography-mass spectrometry (GC-MS) (English Version)
Determination of certain substances in electrical and electronic products—Part 10:Polycyclic aromatic hydrocarbons (PAHs) in polymers and electronics by gas chromatography-mass spectrometry (GC-MS)
GB/T 39560.10-2024 Determination of certain substances in electrical and electronic products - Part 10: Polycyclic aromatic hydrocarbons (PAHs) in polymers and electronics by gas chromatography-mass spectrometry (GC-MS)
1 Scope
This document specifies one normative technique for the determination of polycyclic aromatic hydrocarbons (PAHs) in polymers of electrotechnical products. These PAHs can especially be found in the plastic and rubber parts of a wide range of consumer articles. They are present as impurities in some of the raw materials used in the production of such articles, in particular in extender oils and in carbon black. They are not added intentionally to the articles and do not perform any specific function as constituents of the plastic or rubber parts.
The gas chromatography-mass spectrometry (GC-MS) test method is suitable for the determination of polycyclic aromatic hydrocarbons (PAHs). These test methods have been evaluated for use with plastics and rubbers. These test methods have been evaluated for use with ABS (acrylonitrile butadiene styrene) containing individual PAHs ranging from 37.2 mg/kg to 119 mg/kg and rubbers containing individual PAHs ranging from 1 mg/kg to 221.2 mg/kg.
2 Normative references
The following documents are referred to in the text in such a way that some or all of their content constitutes requirements of this document. For dated references, only the edition cited applies. For undated references, the latest edition of the referenced document (including any amendments) applies.
GB/T 39560.1-2020 Determination of certain substances in electrotechnical products - Part 1: Introduction and overview
ISO 3696 Water for analytical laboratory use - Specification and test methods
3 Terms, definitions and abbreviated terms
3.1 Terms and definitions
No terms and definitions are listed in this document.
ISO and IEC maintain terminological databases for use in standardization at the following
addresses:
——IEC Electropedia: available at http://www.electropedia.org/
——ISO Online browsing platform: available at http://www.iso.org/obp
3.2 Abbreviated terms
ABS: acrylonitrile butadiene styrene
CCC: continuing calibration check standard
EI: electron ionization
GC-MS: gas chromatography-mass spectrometry
IS: internal standard
IUPAC: International Union of Pure and Applied Chemistry
LOD: limit of detection
LOQ: limit of quantification
MDL: method detection limit
PAH: polycyclic aromatic hydrocarbon
PBDE: polybrominated diphenyl ether
QC: quality control
RSD: relative standard deviation
SIM: selected ion monitoring
TICS: tentatively identified compounds
4 Principle
PAH compounds are quantitatively determined using ultrasonic extraction or Soxhlet extraction followed by gas chromatography-mass spectrometry (GC-MS) using single (or "selected") ion monitoring (SIM).
Standard
GB/T 39560.10-2024 Determination of certain substances in electrical and electronic products—Part 10:Polycyclic aromatic hydrocarbons (PAHs) in polymers and electronics by gas chromatography-mass spectrometry (GC-MS) (English Version)
Standard No.
GB/T 39560.10-2024
Status
valid
Language
English
File Format
PDF
Word Count
19000 words
Price(USD)
570.0
Implemented on
2024-12-1
Delivery
via email in 1~3 business day
Detail of GB/T 39560.10-2024
Standard No.
GB/T 39560.10-2024
English Name
Determination of certain substances in electrical and electronic products—Part 10:Polycyclic aromatic hydrocarbons (PAHs) in polymers and electronics by gas chromatography-mass spectrometry (GC-MS)
GB/T 39560.10-2024 Determination of certain substances in electrical and electronic products - Part 10: Polycyclic aromatic hydrocarbons (PAHs) in polymers and electronics by gas chromatography-mass spectrometry (GC-MS)
1 Scope
This document specifies one normative technique for the determination of polycyclic aromatic hydrocarbons (PAHs) in polymers of electrotechnical products. These PAHs can especially be found in the plastic and rubber parts of a wide range of consumer articles. They are present as impurities in some of the raw materials used in the production of such articles, in particular in extender oils and in carbon black. They are not added intentionally to the articles and do not perform any specific function as constituents of the plastic or rubber parts.
The gas chromatography-mass spectrometry (GC-MS) test method is suitable for the determination of polycyclic aromatic hydrocarbons (PAHs). These test methods have been evaluated for use with plastics and rubbers. These test methods have been evaluated for use with ABS (acrylonitrile butadiene styrene) containing individual PAHs ranging from 37.2 mg/kg to 119 mg/kg and rubbers containing individual PAHs ranging from 1 mg/kg to 221.2 mg/kg.
2 Normative references
The following documents are referred to in the text in such a way that some or all of their content constitutes requirements of this document. For dated references, only the edition cited applies. For undated references, the latest edition of the referenced document (including any amendments) applies.
GB/T 39560.1-2020 Determination of certain substances in electrotechnical products - Part 1: Introduction and overview
ISO 3696 Water for analytical laboratory use - Specification and test methods
3 Terms, definitions and abbreviated terms
3.1 Terms and definitions
No terms and definitions are listed in this document.
ISO and IEC maintain terminological databases for use in standardization at the following
addresses:
——IEC Electropedia: available at http://www.electropedia.org/
——ISO Online browsing platform: available at http://www.iso.org/obp
3.2 Abbreviated terms
ABS: acrylonitrile butadiene styrene
CCC: continuing calibration check standard
EI: electron ionization
GC-MS: gas chromatography-mass spectrometry
IS: internal standard
IUPAC: International Union of Pure and Applied Chemistry
LOD: limit of detection
LOQ: limit of quantification
MDL: method detection limit
PAH: polycyclic aromatic hydrocarbon
PBDE: polybrominated diphenyl ether
QC: quality control
RSD: relative standard deviation
SIM: selected ion monitoring
TICS: tentatively identified compounds
4 Principle
PAH compounds are quantitatively determined using ultrasonic extraction or Soxhlet extraction followed by gas chromatography-mass spectrometry (GC-MS) using single (or "selected") ion monitoring (SIM).