1 Scope
This standard specifies the LC-MS-MS determination method of lincomycin, erythromycin, spiramycin, tilmicosin, tylosin, josamycin, kitasamycin, oleandomycin residues in honey.
This standard is applicable to the determination of lincomycin, erythromycin, spiramycin, tilmicosin, tylosin, josamycin, kitasamycin, oleandomycin residues in honey.
For the purpose of this method, the limit of detection is 2.0 μg/kg.
2 Normative references
The following normative documents contain provisions which, through reference in this text, constitute provisions of this standard. For dated references, subsequent amendments (excluding corrections), or revisions, of any of these publications do not apply to this standard. However parties to agreements based on this standard are encouraged to investigate the possibility of applying the most recent editions of the normative documents indicated below. For undated references, the latest edition of the normative document referred to applies.
GB/T 6379.1 Accuracy (trueness and precision) of measurement methods and results - Part 1: General principles and definitions (GB/T 6379.1-2004; ISO 5725-1: 1994, IDT)
GB/T 6379.2 Accuracy (trueness and precision) of measurement methods and results - Part 2: Basic method for the determination of repeatability and reproducibility of a standard measurement method (GB/T 6379.2-2004; ISO 5725-2: 1994, IDT)
GB/T 6682 Water for analytical laboratory use - Specification and test methods (GB/T 6682-2008; ISO 3696: 1987, MOD)
Foreword i
1 Scope
2 Normative references
3 Principle
4 Reagents and materials
5 Instruments
6 Preparation and preservation of specimen
7 Determination procedures
8 Result calculation
9 Precision
Annex A (Informative) Multiple reaction monitoring (MRM) chromatograms of standard substances
Annex B (Informative) Recovery rate
Standard
GB/T 22941-2008 Determination of lincomycin,erythromycin,spiramycin, tilmicosin,tylosin,josamycin,kitasamycin,oleandomycin residues in honey—LC-MS-MS method (English Version)
Standard No.
GB/T 22941-2008
Status
valid
Language
English
File Format
PDF
Word Count
7000 words
Price(USD)
170.0
Implemented on
2009-5-1
Delivery
via email in 1 business day
Detail of GB/T 22941-2008
Standard No.
GB/T 22941-2008
English Name
Determination of lincomycin,erythromycin,spiramycin, tilmicosin,tylosin,josamycin,kitasamycin,oleandomycin residues in honey—LC-MS-MS method
1 Scope
This standard specifies the LC-MS-MS determination method of lincomycin, erythromycin, spiramycin, tilmicosin, tylosin, josamycin, kitasamycin, oleandomycin residues in honey.
This standard is applicable to the determination of lincomycin, erythromycin, spiramycin, tilmicosin, tylosin, josamycin, kitasamycin, oleandomycin residues in honey.
For the purpose of this method, the limit of detection is 2.0 μg/kg.
2 Normative references
The following normative documents contain provisions which, through reference in this text, constitute provisions of this standard. For dated references, subsequent amendments (excluding corrections), or revisions, of any of these publications do not apply to this standard. However parties to agreements based on this standard are encouraged to investigate the possibility of applying the most recent editions of the normative documents indicated below. For undated references, the latest edition of the normative document referred to applies.
GB/T 6379.1 Accuracy (trueness and precision) of measurement methods and results - Part 1: General principles and definitions (GB/T 6379.1-2004; ISO 5725-1: 1994, IDT)
GB/T 6379.2 Accuracy (trueness and precision) of measurement methods and results - Part 2: Basic method for the determination of repeatability and reproducibility of a standard measurement method (GB/T 6379.2-2004; ISO 5725-2: 1994, IDT)
GB/T 6682 Water for analytical laboratory use - Specification and test methods (GB/T 6682-2008; ISO 3696: 1987, MOD)
Contents of GB/T 22941-2008
Foreword i
1 Scope
2 Normative references
3 Principle
4 Reagents and materials
5 Instruments
6 Preparation and preservation of specimen
7 Determination procedures
8 Result calculation
9 Precision
Annex A (Informative) Multiple reaction monitoring (MRM) chromatograms of standard substances
Annex B (Informative) Recovery rate