Standard No.:	GB/T 23972-2009
English Name:	Determination of alkylphenols and alkylphenol polyethoxylates in textile dyeing and finishing auxiliaries—LC/MS method
Chinese Name:	纺织染整助剂中烷基苯酚及烷基苯酚聚氧乙烯醚的测定 高效液相色谱/质谱法
Chinese Classification:	G70    Basic standards and general methods for chemical additive
Professional Classification:	GB    National Standard
ICS Classification:	71.100.40 71.100.40    Surface active agents 71.100.40
Issued by:	CPCIA
Issued on:	2009-6-2
Implemented on:	2010-2-1
Status:	valid
Language:	English
File Format:	PDF
Word Count:	6000 words
Price(USD):	140.0
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1 Scope This standard specifies the determination method of alkylphenols and alkylphenol polyethoxylates in textile dyeing and finishing auxiliaries. This standard is applicable to the determination of alkylphenol and alkylphenol polyethoxylate in textile dyeing and finishing auxiliaries with LC/MS method. 2 Normative References The following clauses in the document constitute provisions of this standard through quoting it. The following normative documents contain provisions which, through reference in this text, constitute provisions of this standard. For dated reference, subsequent amendments (excluding corrections) to, or revisions of, any of these publications do not apply. However, parties to agreements based on this standard are encouraged to investigate the possibility of applying the most recent editions of the standards indicated below. For undated references, the latest edition applies. GB/T 6682-2008 Water for Analytical Laboratory Use - Specification and Test Methods (ISO 3696: 1987, MOD) GB/T 8170-2008 Rules of Rounding off for Numerical Values & Expression and Judgment of Limiting Values 3 Terms and Definitions For the purposes of this standard, the following terms and definitions apply. 3.1 alkylphenols, referred to as AP the molecular structure of alkylphenols is: R-C6H4-OH. Common substances of this class are octylphenol (C8H17-C6H4-OH, referred to as OP) and nonylphenol (C9H19-C5H4-OH, referred to as NP) 3.2 alkylphenol polyethoxylates, referred to as APEO the molecular structure formula of alkylphenol polyethoxylates is: R-C6H4-(OC2H4)nOH. Common substances of this class are octylphenol ethoxylate [C8H17-C6H4-(OC2H4)nOH], referred to as OPEO and nonylphenol ethoxylate [C9H19-C6H4-(OC2H4)nOH], referred to as NPEO Alkylphenol polyethoxylates can be used as the surfactant in textile dyeing and finishing auxiliaries, and alkylphenols are degradation products of alkylphenol polyethoxylates 4 Determination Method

Foreword i 1 Scope 2 Normative References 3 Terms and Definitions 4 Determination Method 5 Detection Lower Limit, Recovery Rate and Precision 6 Test Report Annex A (Normative) CAS RN of Common OP, NP, OPEO and NPEO Annex B (Informative) Schematic Diagrams