无损检测 磁粉检测用材料
Non-destructive testing - Materials for magnetic particle testing
1 范围
1 Scope
本标准规定了磁粉检测用材料(或检测介质，包括磁悬液、干磁粉、载液、反差增强剂)的分类、技术要求和检验方法等。
This standard specifies the classification, technical requirements and inspection methods of materials (or testing medium, including magnetic ink, dry magnetic powders, carrier fluid and contrast aid paints) for magnetic particle testing.
本标准适用于检测介质的型式检验和批量检验。
This standard is applicable to type inspection and batch inspection of testing medium.
本标准也可作为用户订货的验收依据。
It may also be used as the basis for acceptance of user orders.
2 规范性引用文件
2 Normative references
下列文件中的条款通过本标准的引用而成为本标准的条款。凡是注日期的引用文件，其随后所有的修改单(不包括勘误的内容)或修订版均不适用于本标准，然而，鼓励根据本标准达成协议的各方研究是否可使用这些文件的最新版本。凡是不注日期的引用文件，其最新版本适用于本标准。
The following normative documents contain provisions which, through reference in this text, constitute provisions of this standard. For dated references, subsequent amendments (excluding corrections), or revisions, of any of these publications do not apply to this standard. However parties to agreements based on this standard are encouraged to investigate the possibility of applying the most recent editions of the normative documents indicated below. For undated references, the latest edition applies.
GB/T 265 石油产品运动粘度测定法和动力粘度计算法
Petroleum products - Determination of kinematic viscosity and calculation of dynamic viscosity
GB/T 699 优质碳素结构钢
Quality carbon structure steels
GB/T 2007.7 散装矿产品取样、制样通则 粒度测定方法 手工筛分法(GB/T 2007.7—1987，neq ISO 2591：1982)
General rules for the sampling and sample preparation of minerals in bulk - The method for determination of size by manual sieving (GB/T 2007.7-1987, neq ISO 2591:1982)
GB/T 5097 无损检测 渗透检测和磁粉检测 观察条件(GB/T 5097—2005，ISO 3059：2001，IDT)
Non-destructive testing - Penetrant testing and magnetic particle testing - Viewing conditions (GB/T 5097-2005, ISO 3059: 2001, IDT)
GB/T 6368 表面活性剂 水溶液pH值的测定 电位法(GB/T 6368—1993，eqv ISO 4316：1977)
Surface active agents - Determination of pH of aqueous solution - Potentiometric method (GB/T 6368-1993, eqv ISO 4316:1977)
GB/T 8034 焦化苯类产品铜片腐蚀的测定方法(GB/T 8034—1987，eqv ISO 2160：1972)
Benzol products of coal carbonization - Corrosiveness to copper - Copper strip test (GB/T 8034-1987, eqv ISO 2160:1972)
GB/T 12604.5 无损检测术语 磁粉检测
Non-destructive testing - Terminology - Terms used in magnetic particle testing
GB/T 15822(所有部分)
GB/T 15822 (All parts) 无损检测 磁粉检测(GB/T 15822.1～3—2005，ISO 9934-1：2001，ISO 9934-2～3：2002，IDT)
Non-destructive testing - Magnetic particle testing (GB/T 15822.1~3-2005, ISO 9934-1:2001, ISO 9934-2~3:2002, IDT)
JB/T 7523-2004 无损检测 渗透检测用材料
Non-destructive testing - Materials for penetrant testing
3 术语和定义
3 Terms and definitions
GB/T 12604.5中确立的术语和定义适用于本标准。
For the purpose of this standard, the terms and definitions established in GB/T 12604.5 apply.
4 安全预防
4 Safety precautions
磁粉检测用材料及其检验用的化学制品，可能是有害的、易燃的和(或)易挥发的，因此宜遵守各项规定的预防措施。应遵守国家和地方颁布的所有关于安全卫生、环保要求的法规。
Materials for magnetic particle testing and chemicals for inspection may be harmful, flammable and/or volatile, so the precautions should be followed. All national and local laws and regulations on safety, sanitation and environmental protection shall be observed.
Contents
前言 Foreword i
1 范围 1 Scope
2 规范性引用文件 2 Normative references
3 术语和定义 3 Terms and definitions
4 安全预防 4 Safety precautions
5 分类 5 Classification
5.1 概述 5.1 General
5.2 磁悬液 5.2 Magnetic ink
5.3 干磁粉 5.3 Dry magnetic powder
6 检验规则 6 Inspection rules
6.1 组批规则 6.1 Batching rules
6.2 检验分类 6.2 Inspection classification
6.3 检验项目 6.3 Inspection items
7 检验方法和技术要求 7 Inspection methods and technical requirements
7.1 性能 7.1 Performance
7.2 颜色 7.2 Color
7.3 磁粉尺寸 7.3 Magnetic particle size
7.4 耐热性 7.4 Heat resistance
7.5 荧光系数和荧光稳定性 7.5 Fluorescence index and fluorescence stability
7.6 载液的荧光 7.6 Fluorescence of carrier fluid
7.7 闪点 7.7 Flash point
7.8 检测介质引起的腐蚀 7.8 Corrosion caused by testing medium
7.9 载液的粘度 7.9 Viscosity of carrier fluid
7.10 机械稳定性 7.10 Mechanical stability
7.11 起泡 7.11 Bubbling
7.12 pH值 7.12 pH value
7.13 贮存稳定性 7.13 Storage stability
7.14 固体含量 7.14 Solid content
7.15 硫及卤素含量 7.15 Sulfur and halogen content
8 标志和标签 8 Mark and Label
9 包装、运输和贮存 9 Packaging, transportation and storage
附录A (规范性附录) 型式和批量检验规程 Annex A (Normative) Type and batch inspection specifications
A.1 检测介质的准备 A.1 Preparation of testing medium
A.2 参考试块的清洗 A.2 Cleaning of reference block
A.3 检测介质的施加 A.3 Application of testing medium
A.4 检验与解释 A.4 Inspection and interpretation
A.4.1 检验 A.4.1 Inspection
A.4.2 解释 A.4.2 Interpretation
A.5 反差增强剂 A.5 Contrast aid paints
附录B (规范性附录) 参考试块 Annex B (Normative) Reference block
B.1 1型参考试块 B.1 Type 1 reference block
B.1.1 简述 B.1.1 Brief description
B.1.2 制造 B.1.2 Fabrication
B.1.3 验证 B.1.3 Verification
B.2 2型参考试块 B.2 Type 2 reference block
B.2.1 简述 B.2.1 Brief description
B.2.2 制造 B.2.2 Fabrication
B.2.3 验证 B.2.3 Verification
附录C (规范性附录) 钢腐蚀检验 Annex C (Normative) Inspection of corrosiveness to steel
C.1 原则 C.1 Principles
C.2 装置 C.2 Apparatus
C.3 试剂和材料 C.3 Reagents and materials
C.4 检验步骤 C.4 Inspection steps
C.4.1 溶液制备(100mL) C.4.1 Preparation of solutions (100mL)
C.4.2 铁粒与过滤纸的制备 C.4.2 Preparation of iron particles and filter paper
C.4.3 腐蚀检验 C.4.3 Corrosion inspection
C.5 结果解释 C.5 Interpretation of results
C.6 结果表述 C.6 Expression of results
C.7 不确定性 C.7 Uncertainty
参考文献 Bibliography
图1 磁粉荧光系数β的测定 Figure 1 Determination for fluorescence index β of magnetic particles
图2 7.10.2的搅拌布置结构 Figure 2 Structure of stirring apparatus in 7.10.2
图B.1 1型参考试块 Figure B.1 Type 1 reference block
图B.2 2型参考试块 Figure B.2 Type 2 reference block
图B.3 插入磁体的示意图 Figure B.3 Schematic diagram for inserting magnet
图B.4 2型试块的刻槽 Figure B.4 Grooving of Type 2 test block
图C.1 腐蚀痕迹的评价 Figure C.1 Evaluation of corrosion traces
表1 磁粉材料的检验 Table 1 Inspection of materials for magnetic particle testing
表C.1 过滤纸上腐蚀污染分级 Table C.1 Grading of corrosion contamination on filter paper
无损检测 磁粉检测用材料
Non-destructive testing - Materials for magnetic particle testing
1 范围
1 Scope
本标准规定了磁粉检测用材料(或检测介质，包括磁悬液、干磁粉、载液、反差增强剂)的分类、技术要求和检验方法等。
This standard specifies the classification, technical requirements and inspection methods of materials (or testing medium, including magnetic ink, dry magnetic powders, carrier fluid and contrast aid paints) for magnetic particle testing.
本标准适用于检测介质的型式检验和批量检验。
This standard is applicable to type inspection and batch inspection of testing medium.
本标准也可作为用户订货的验收依据。
It may also be used as the basis for acceptance of user orders.
2 规范性引用文件
2 Normative references
下列文件中的条款通过本标准的引用而成为本标准的条款。凡是注日期的引用文件，其随后所有的修改单(不包括勘误的内容)或修订版均不适用于本标准，然而，鼓励根据本标准达成协议的各方研究是否可使用这些文件的最新版本。凡是不注日期的引用文件，其最新版本适用于本标准。
The following normative documents contain provisions which, through reference in this text, constitute provisions of this standard. For dated references, subsequent amendments (excluding corrections), or revisions, of any of these publications do not apply to this standard. However parties to agreements based on this standard are encouraged to investigate the possibility of applying the most recent editions of the normative documents indicated below. For undated references, the latest edition applies.
GB/T 265 石油产品运动粘度测定法和动力粘度计算法
Petroleum products - Determination of kinematic viscosity and calculation of dynamic viscosity
GB/T 699 优质碳素结构钢
Quality carbon structure steels
GB/T 2007.7 散装矿产品取样、制样通则 粒度测定方法 手工筛分法(GB/T 2007.7—1987，neq ISO 2591：1982)
General rules for the sampling and sample preparation of minerals in bulk - The method for determination of size by manual sieving (GB/T 2007.7-1987, neq ISO 2591:1982)
GB/T 5097 无损检测 渗透检测和磁粉检测 观察条件(GB/T 5097—2005，ISO 3059：2001，IDT)
Non-destructive testing - Penetrant testing and magnetic particle testing - Viewing conditions (GB/T 5097-2005, ISO 3059: 2001, IDT)
GB/T 6368 表面活性剂 水溶液pH值的测定 电位法(GB/T 6368—1993，eqv ISO 4316：1977)
Surface active agents - Determination of pH of aqueous solution - Potentiometric method (GB/T 6368-1993, eqv ISO 4316:1977)
GB/T 8034 焦化苯类产品铜片腐蚀的测定方法(GB/T 8034—1987，eqv ISO 2160：1972)
Benzol products of coal carbonization - Corrosiveness to copper - Copper strip test (GB/T 8034-1987, eqv ISO 2160:1972)
GB/T 12604.5 无损检测术语 磁粉检测
Non-destructive testing - Terminology - Terms used in magnetic particle testing
GB/T 15822(所有部分)
GB/T 15822 (All parts) 无损检测 磁粉检测(GB/T 15822.1～3—2005，ISO 9934-1：2001，ISO 9934-2～3：2002，IDT)
Non-destructive testing - Magnetic particle testing (GB/T 15822.1~3-2005, ISO 9934-1:2001, ISO 9934-2~3:2002, IDT)
JB/T 7523-2004 无损检测 渗透检测用材料
Non-destructive testing - Materials for penetrant testing
3 术语和定义
3 Terms and definitions
GB/T 12604.5中确立的术语和定义适用于本标准。
For the purpose of this standard, the terms and definitions established in GB/T 12604.5 apply.
4 安全预防
4 Safety precautions
磁粉检测用材料及其检验用的化学制品，可能是有害的、易燃的和(或)易挥发的，因此宜遵守各项规定的预防措施。应遵守国家和地方颁布的所有关于安全卫生、环保要求的法规。
Materials for magnetic particle testing and chemicals for inspection may be harmful, flammable and/or volatile, so the precautions should be followed. All national and local laws and regulations on safety, sanitation and environmental protection shall be observed.
Contents of JB/T 6063-2006
Contents
前言 Foreword i
1 范围 1 Scope
2 规范性引用文件 2 Normative references
3 术语和定义 3 Terms and definitions
4 安全预防 4 Safety precautions
5 分类 5 Classification
5.1 概述 5.1 General
5.2 磁悬液 5.2 Magnetic ink
5.3 干磁粉 5.3 Dry magnetic powder
6 检验规则 6 Inspection rules
6.1 组批规则 6.1 Batching rules
6.2 检验分类 6.2 Inspection classification
6.3 检验项目 6.3 Inspection items
7 检验方法和技术要求 7 Inspection methods and technical requirements
7.1 性能 7.1 Performance
7.2 颜色 7.2 Color
7.3 磁粉尺寸 7.3 Magnetic particle size
7.4 耐热性 7.4 Heat resistance
7.5 荧光系数和荧光稳定性 7.5 Fluorescence index and fluorescence stability
7.6 载液的荧光 7.6 Fluorescence of carrier fluid
7.7 闪点 7.7 Flash point
7.8 检测介质引起的腐蚀 7.8 Corrosion caused by testing medium
7.9 载液的粘度 7.9 Viscosity of carrier fluid
7.10 机械稳定性 7.10 Mechanical stability
7.11 起泡 7.11 Bubbling
7.12 pH值 7.12 pH value
7.13 贮存稳定性 7.13 Storage stability
7.14 固体含量 7.14 Solid content
7.15 硫及卤素含量 7.15 Sulfur and halogen content
8 标志和标签 8 Mark and Label
9 包装、运输和贮存 9 Packaging, transportation and storage
附录A (规范性附录) 型式和批量检验规程 Annex A (Normative) Type and batch inspection specifications
A.1 检测介质的准备 A.1 Preparation of testing medium
A.2 参考试块的清洗 A.2 Cleaning of reference block
A.3 检测介质的施加 A.3 Application of testing medium
A.4 检验与解释 A.4 Inspection and interpretation
A.4.1 检验 A.4.1 Inspection
A.4.2 解释 A.4.2 Interpretation
A.5 反差增强剂 A.5 Contrast aid paints
附录B (规范性附录) 参考试块 Annex B (Normative) Reference block
B.1 1型参考试块 B.1 Type 1 reference block
B.1.1 简述 B.1.1 Brief description
B.1.2 制造 B.1.2 Fabrication
B.1.3 验证 B.1.3 Verification
B.2 2型参考试块 B.2 Type 2 reference block
B.2.1 简述 B.2.1 Brief description
B.2.2 制造 B.2.2 Fabrication
B.2.3 验证 B.2.3 Verification
附录C (规范性附录) 钢腐蚀检验 Annex C (Normative) Inspection of corrosiveness to steel
C.1 原则 C.1 Principles
C.2 装置 C.2 Apparatus
C.3 试剂和材料 C.3 Reagents and materials
C.4 检验步骤 C.4 Inspection steps
C.4.1 溶液制备(100mL) C.4.1 Preparation of solutions (100mL)
C.4.2 铁粒与过滤纸的制备 C.4.2 Preparation of iron particles and filter paper
C.4.3 腐蚀检验 C.4.3 Corrosion inspection
C.5 结果解释 C.5 Interpretation of results
C.6 结果表述 C.6 Expression of results
C.7 不确定性 C.7 Uncertainty
参考文献 Bibliography
图1 磁粉荧光系数β的测定 Figure 1 Determination for fluorescence index β of magnetic particles
图2 7.10.2的搅拌布置结构 Figure 2 Structure of stirring apparatus in 7.10.2
图B.1 1型参考试块 Figure B.1 Type 1 reference block
图B.2 2型参考试块 Figure B.2 Type 2 reference block
图B.3 插入磁体的示意图 Figure B.3 Schematic diagram for inserting magnet
图B.4 2型试块的刻槽 Figure B.4 Grooving of Type 2 test block
图C.1 腐蚀痕迹的评价 Figure C.1 Evaluation of corrosion traces
表1 磁粉材料的检验 Table 1 Inspection of materials for magnetic particle testing
表C.1 过滤纸上腐蚀污染分级 Table C.1 Grading of corrosion contamination on filter paper
