1 Scope
This standard specifies LC-MS-MS method for determination of streptomycin, dihydrostreptomycin and kanamycin residues in royal jelly.
This standard is applicable to determination of streptomycin, dihydrostreptomycin and kanamycin residues in royal jelly.
Method detection limit in this standard: detection limit for streptomycin, dihydrostreptomycin and kanamycin is 10.0μg/kg.
2 Normative References
The following normative documents contain provisions which, through reference in this text, constitute provisions of this standard. For dated references, subsequent amendments (excluding corrections), or revisions, of any of these publications do not apply to this standard. However parties to agreements based on this standard are encouraged to investigate the possibility of applying the most recent editions of the normative documents indicated below. For undated references, the latest edition of the normative document referred to applies.
GB/T 6379.1 Accuracy (Trueness and Precision) of Measurement Methods and Results - Part 1: General Principles and Definitions (GB/T 6379.1-2004, ISO 5725-1; 1994, IDT)
GB/T 6379.2 Accuracy (Trueness and Precision) of Measurement Methods and Results - Part 2: Basic Method for the Determination of Repeatability and Reproducibility of a Standard Measurement Method (GB/T 6379.2-2004, ISO 5725-2:1994, IDT)
GB/T 6682 Water for Analytical Laboratory Use-Specification and Test Methods (GB/T 6682-2008, ISO 3696:1987, MOD)
3 Principle
Foreword i
1 Scope
2 Normative References
3 Principle
4 Reagents and Materials
5 Instruments
6 Preparation and Preservation of Specimen
7 Determination Procedures
8 Result Calculation
9 Precision
Annex A (Informative) Multiple Reaction Monitoring (MRM) Chromatogram
Annex B (Informative) Recovery Rate
Standard
GB/T 22945-2008 Determination of streptomycin,dihydrostreptomycin and kanamycin residues in royal jelly—LC-MS-MS method (English Version)
Standard No.
GB/T 22945-2008
Status
valid
Language
English
File Format
PDF
Word Count
3000 words
Price(USD)
184.0
Implemented on
2009-5-1
Delivery
via email in 1 business day
Detail of GB/T 22945-2008
Standard No.
GB/T 22945-2008
English Name
Determination of streptomycin,dihydrostreptomycin and kanamycin residues in royal jelly—LC-MS-MS method
1 Scope
This standard specifies LC-MS-MS method for determination of streptomycin, dihydrostreptomycin and kanamycin residues in royal jelly.
This standard is applicable to determination of streptomycin, dihydrostreptomycin and kanamycin residues in royal jelly.
Method detection limit in this standard: detection limit for streptomycin, dihydrostreptomycin and kanamycin is 10.0μg/kg.
2 Normative References
The following normative documents contain provisions which, through reference in this text, constitute provisions of this standard. For dated references, subsequent amendments (excluding corrections), or revisions, of any of these publications do not apply to this standard. However parties to agreements based on this standard are encouraged to investigate the possibility of applying the most recent editions of the normative documents indicated below. For undated references, the latest edition of the normative document referred to applies.
GB/T 6379.1 Accuracy (Trueness and Precision) of Measurement Methods and Results - Part 1: General Principles and Definitions (GB/T 6379.1-2004, ISO 5725-1; 1994, IDT)
GB/T 6379.2 Accuracy (Trueness and Precision) of Measurement Methods and Results - Part 2: Basic Method for the Determination of Repeatability and Reproducibility of a Standard Measurement Method (GB/T 6379.2-2004, ISO 5725-2:1994, IDT)
GB/T 6682 Water for Analytical Laboratory Use-Specification and Test Methods (GB/T 6682-2008, ISO 3696:1987, MOD)
3 Principle
Contents of GB/T 22945-2008
Foreword i
1 Scope
2 Normative References
3 Principle
4 Reagents and Materials
5 Instruments
6 Preparation and Preservation of Specimen
7 Determination Procedures
8 Result Calculation
9 Precision
Annex A (Informative) Multiple Reaction Monitoring (MRM) Chromatogram
Annex B (Informative) Recovery Rate