GB/T 22964-2008 Determination of lincomycin, oleandomycin, erythromycin, tilmicosin, tylosin, spiramycin, kitasamycin and josamycin residues in fugu and eel - LC-MS-MS method (English Version)
Determination of lincomycin, oleandomycin, erythromycin, tilmicosin, tylosin, spiramycin, kitasamycin and josamycin residues in fugu and eel - LC-MS-MS method
1 Scope
This standard specifies the LC-MS-MS method for the determination of lincomycin, oleandomycin, erythromycin, tilmicosin, tylosin, spiramycin, kitasamycin and josamycin residues in fugu and eel.
This standard is applicable to the determination of lincomycin, oleandomycin, erythromycin, tilmicosin, tylosin, spiramycin, kitasamycin and josamycin residues in fugu and eel.
Method detection limit of this standard: 2.0μg/kg for lincomycin, oleandomycin, erythromycin, tilmicosin, tylosin, spiramycin, kitasamycin and josamycin in fugu; 2.0μg/kg for lincomycin, erythromycin, tylosin and kitasamycin and 5.0μg/kg for spiramycin, oleandomycin, josamycin and tilmicosin in eel.
2 Normative references
The following normative documents contain provisions which, through reference in this text, constitute provisions of this standard. For dated references, subsequent amendments (excluding corrections), or revisions, of any of these publications do not apply to this standard, however parties to agreements based on this standard are encouraged to investigate the possibility of applying the most recent editions of the normative documents indicated below. For undated references, the latest edition applies.
GB/T 6379.1 Accuracy (trueness and precision) of measurement methods and results - Part 1: General principles and definitions (GB/T 6379.1-2004, ISO 5725-1:1994, IDT)
GB/T 6379.2 Accuracy (trueness and precision) of measurement methods and results - Part 2: Basic method for the determination of repeatability and reproducibility of a standard measurement method (GB/T 6379.2-2004, ISO 5725-2:1994, IDT)
GB/T 6682 Water for analytical laboratory use - Specification and test methods (GB/T 6682-2008, ISO 3696:1987, MOD)
3 Principle
Foreword i
1 Scope
2 Normative references
3 Principle
4 Reagents and materials
5 Instruments
6 Specimen preparation and preservation
7 Determination steps
8 Result calculation
9 Precision
Annex A (Informative) Multi-reaction monitoring (MRM) chromatograms of standard substances
Annex B (Informative) Recovery rate
Standard
GB/T 22964-2008 Determination of lincomycin, oleandomycin, erythromycin, tilmicosin, tylosin, spiramycin, kitasamycin and josamycin residues in fugu and eel - LC-MS-MS method (English Version)
Standard No.
GB/T 22964-2008
Status
valid
Language
English
File Format
PDF
Word Count
6000 words
Price(USD)
150.0
Implemented on
2009-5-1
Delivery
via email in 1 business day
Detail of GB/T 22964-2008
Standard No.
GB/T 22964-2008
English Name
Determination of lincomycin, oleandomycin, erythromycin, tilmicosin, tylosin, spiramycin, kitasamycin and josamycin residues in fugu and eel - LC-MS-MS method
1 Scope
This standard specifies the LC-MS-MS method for the determination of lincomycin, oleandomycin, erythromycin, tilmicosin, tylosin, spiramycin, kitasamycin and josamycin residues in fugu and eel.
This standard is applicable to the determination of lincomycin, oleandomycin, erythromycin, tilmicosin, tylosin, spiramycin, kitasamycin and josamycin residues in fugu and eel.
Method detection limit of this standard: 2.0μg/kg for lincomycin, oleandomycin, erythromycin, tilmicosin, tylosin, spiramycin, kitasamycin and josamycin in fugu; 2.0μg/kg for lincomycin, erythromycin, tylosin and kitasamycin and 5.0μg/kg for spiramycin, oleandomycin, josamycin and tilmicosin in eel.
2 Normative references
The following normative documents contain provisions which, through reference in this text, constitute provisions of this standard. For dated references, subsequent amendments (excluding corrections), or revisions, of any of these publications do not apply to this standard, however parties to agreements based on this standard are encouraged to investigate the possibility of applying the most recent editions of the normative documents indicated below. For undated references, the latest edition applies.
GB/T 6379.1 Accuracy (trueness and precision) of measurement methods and results - Part 1: General principles and definitions (GB/T 6379.1-2004, ISO 5725-1:1994, IDT)
GB/T 6379.2 Accuracy (trueness and precision) of measurement methods and results - Part 2: Basic method for the determination of repeatability and reproducibility of a standard measurement method (GB/T 6379.2-2004, ISO 5725-2:1994, IDT)
GB/T 6682 Water for analytical laboratory use - Specification and test methods (GB/T 6682-2008, ISO 3696:1987, MOD)
3 Principle
Contents of GB/T 22964-2008
Foreword i
1 Scope
2 Normative references
3 Principle
4 Reagents and materials
5 Instruments
6 Specimen preparation and preservation
7 Determination steps
8 Result calculation
9 Precision
Annex A (Informative) Multi-reaction monitoring (MRM) chromatograms of standard substances
Annex B (Informative) Recovery rate