1 Scope
In this standard, Method I specifies the determination method of content of 16 phthalate esters in foods via gas chromatography-mass spectrometry (GC-MS) and Method II specifies the determination method of content of 18 phthalate esters in foods via gas chromatography-mass spectrometry (GC-MS).
In this standard, Method I is applicable to the determination and confirmation of content of dimethyl phthalate (DMP), diethyl phthalate (DEP), diisobutyl phthalate (DIBP), dibutyl phthalate (DBP), bis(2-methoxyethyl) phthalate (DMEP), bis(4-methyl-2-pentyl) phthalate (BMPP), bis(2-ethoxyethyl) phthalate (DEEP), dipentyl phthalate (DPP), dihexyl phthalate (DHXP), benzyl butyl phthalate (BBP), bis(2-n-butoxyethyl) phthalate (DBEP), dicyclohexyl phthalate (DCHP), bis(2-ethylhexyl) phthalate (DEHP), diphenyl phthalate (DPhP), di-n-octyl phthalate (DNOP) or dinonyl phthalate (DNP) in foods via internal standard method, and Method II is applicable to determination and confirmation of content of dimethyl phthalate (DMP), diethyl phthalate (DEP), diallyl phthalate (DAP), diisobutyl phthalate (DIBP), dibutyl phthalate (DBP), bis(2-methoxyethyl) phthalate (DMEP), bis(4-methyl-2-pentyl) phthalate (BMPP), bis(2-ethoxyethyl) phthalate (DEEP), dipentyl phthalate (DPP), dihexyl phthalate (DHXP), benzyl butyl phthalate (BBP), bis(2-n-butoxyethyl) phthalate (DBEP), dicyclohexyl phthalate (DCHP), bis(2-ethylhexyl) phthalate (DEHP), diphenyl phthalate (DPhP), di-n-octyl phthalate (DNOP), diisononyl ortho-phthalate (DINP) or dinonyl phthalate (DNP) in foods via external standard method.
Method I Gas Chromatography - Mass Spectrometry:
Isotope Internal Standard Method
2 Principle
Foreword i
1 Scope
2 Principle
3 Reagents and Materials
4 Instruments and Apparatus
5 Analysis Steps
6 Expression of Analysis Results
7 Precision
8 Miscellaneous
9 Principle
10 Reagents and Materials
11 Instruments and Apparatus
12 Analysis Steps
13 Expression of Analysis Results
14 Precision
15 Miscellaneous
Annex A Table of Information on Common Phthalate Plasticizers
Annex B Monitored Ion Parameters of Phthalates in Isotope Internal Standard Method
Annex C Total Ion Chromatogram of Phthalate Standard Solutions (Isotope Internal Standard Method)
Annex D Monitored Ion Parameters of Phthalates in External Standard Method
Annex E Total Ion Chromatogram of Phthalate Standard Solutions (External Standard Method)
Standard
GB 5009.271-2016 National Food Safety Standard - Determination of Phthalates in Food (English Version)
Standard No.
GB 5009.271-2016
Status
valid
Language
English
File Format
PDF
Word Count
4000 words
Price(USD)
80.0
Implemented on
2017-6-23
Delivery
via email in 1 business day
Detail of GB 5009.271-2016
Standard No.
GB 5009.271-2016
English Name
National Food Safety Standard - Determination of Phthalates in Food
Chinese Name
食品安全国家标准 食品中邻苯二甲酸酯的测定
Chinese Classification
Professional Classification
GB
ICS Classification
Issued by
National Health and Family Planning Commission, China Food and Drug Administration
1 Scope
In this standard, Method I specifies the determination method of content of 16 phthalate esters in foods via gas chromatography-mass spectrometry (GC-MS) and Method II specifies the determination method of content of 18 phthalate esters in foods via gas chromatography-mass spectrometry (GC-MS).
In this standard, Method I is applicable to the determination and confirmation of content of dimethyl phthalate (DMP), diethyl phthalate (DEP), diisobutyl phthalate (DIBP), dibutyl phthalate (DBP), bis(2-methoxyethyl) phthalate (DMEP), bis(4-methyl-2-pentyl) phthalate (BMPP), bis(2-ethoxyethyl) phthalate (DEEP), dipentyl phthalate (DPP), dihexyl phthalate (DHXP), benzyl butyl phthalate (BBP), bis(2-n-butoxyethyl) phthalate (DBEP), dicyclohexyl phthalate (DCHP), bis(2-ethylhexyl) phthalate (DEHP), diphenyl phthalate (DPhP), di-n-octyl phthalate (DNOP) or dinonyl phthalate (DNP) in foods via internal standard method, and Method II is applicable to determination and confirmation of content of dimethyl phthalate (DMP), diethyl phthalate (DEP), diallyl phthalate (DAP), diisobutyl phthalate (DIBP), dibutyl phthalate (DBP), bis(2-methoxyethyl) phthalate (DMEP), bis(4-methyl-2-pentyl) phthalate (BMPP), bis(2-ethoxyethyl) phthalate (DEEP), dipentyl phthalate (DPP), dihexyl phthalate (DHXP), benzyl butyl phthalate (BBP), bis(2-n-butoxyethyl) phthalate (DBEP), dicyclohexyl phthalate (DCHP), bis(2-ethylhexyl) phthalate (DEHP), diphenyl phthalate (DPhP), di-n-octyl phthalate (DNOP), diisononyl ortho-phthalate (DINP) or dinonyl phthalate (DNP) in foods via external standard method.
Method I Gas Chromatography - Mass Spectrometry:
Isotope Internal Standard Method
2 Principle
Contents of GB 5009.271-2016
Foreword i
1 Scope
2 Principle
3 Reagents and Materials
4 Instruments and Apparatus
5 Analysis Steps
6 Expression of Analysis Results
7 Precision
8 Miscellaneous
9 Principle
10 Reagents and Materials
11 Instruments and Apparatus
12 Analysis Steps
13 Expression of Analysis Results
14 Precision
15 Miscellaneous
Annex A Table of Information on Common Phthalate Plasticizers
Annex B Monitored Ion Parameters of Phthalates in Isotope Internal Standard Method
Annex C Total Ion Chromatogram of Phthalate Standard Solutions (Isotope Internal Standard Method)
Annex D Monitored Ion Parameters of Phthalates in External Standard Method
Annex E Total Ion Chromatogram of Phthalate Standard Solutions (External Standard Method)