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Position: Chinese Standard in English/GB/T 601-2016
GB/T 601-2016   Chemical Reagent - Preparations of Standard Volumetric Solutions (English Version)
Standard No.: GB/T 601-2016 Status:valid remind me the status change

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Language:English File Format:PDF
Word Count: 22500 words Price(USD):280.0 remind me the price change

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Implemented on:2017-5-1 Delivery: via email in 1 business day
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Standard No.: GB/T 601-2016
English Name: Chemical Reagent - Preparations of Standard Volumetric Solutions
Chinese Name: 化学试剂 标准滴定溶液的制备
Professional Classification: GB    National Standard
ICS Classification: 71.040.40 71.040.40    Chemical analysis 71.040.40
Issued by: AQSIQ,SAC
Issued on: 2016-10-13
Implemented on: 2017-5-1
Status: valid
Superseding:GB/T 601-2002 Chemical Reagent - Preparations of Standard Volumetric Solutions
Language: English
File Format: PDF
Word Count: 22500 words
Price(USD): 280.0
Delivery: via email in 1 business day
1 Scope This standard specifies preparation and calibration method of chemical reagent reference titration solution. This standard is applicable to both preparation and calibration of reference titration solution whose chemical reagent purity and impurity content is determined by titration and other areas. 2 Normative References The following documents for the application of this document are essential. For dated reference, only the edition cited applies. For undated references, the latest edition (including any amendments) applies. GB/T 603 Chemical Reagent - Preparations of Reagent Solutions for Use in Test Method GB/T 606 Chemical Reagent - General Method for the Determination of Water - Karl Fischer Method GB/T 6379.6-2009 Accuracy(trueness and precision) of Measurement Methods and Results - Part 6: Use in Practice of Accuracy Values GB/T 6682 Water for Analytical Laboratory Use-Specification and Test Methods GB/T 9725-2007 Chemical Reagent - General Rule for Potentiometric Titration JJG 130 Verification Regulation of Liquid-in-Glass Thermometers for Working JJG 196-2006 Verification Regulation of Working Glass Container JJG 1036 Verification Regulation for Electronic Balance 3 General Requirements 3.1 Unless otherwise specified in this standard, the analytically pure level and above reagents, preparations and products prepared according to GB/T 603 and Grade 3 water (defined in GB/T 6682) shall be adopted for the purpose of this standard. 3.2 The concentration of reference titration solution prepared in this standard refers to that at 20℃ except perchloric acid reference titration solution, hydrochloric acid-ethanol reference titration solution and sodium nitrite reference titration solution [c(NaNO2)=0.5 mol/L]. If calibration, direct preparation and use of reference titration solution is not conducted at 20℃, volume of shall be corrected (see Annex A). Reference titration solution with "calibration prior to use" may not be corrected in case of not large temperature difference during calibration and use. Calibration, direct preparation and analytical balance, burette, one-mark volumetric flask and one-mark pipet for use shall be verified or calibrated periodically according to relevant verification regulation and determination method of burette volume is performed according to Annex B. Besides, one-mark volumetric flask and one-mark pipet shall be provided with volume correction factor.
Foreword i 1 Scope 2 Normative References 3 General Requirements 4 Preparation and Calibration of Reference Titration Solution 4.1 Sodium Hydroxide Reference Titration Solution 4.2 Hydrochloric Acid Reference Titration Solution 4.3 Sulfuric Acid Reference Titration Solution 4.4 Sodium Carbonate Reference Titration Solution 4.5 Potassium Bichromate Reference Titration Solution [c(1/6 K2Cr2O7)=0.1 mol/L] 4.6 Sodium Thiosulfate Reference Titration Solution [c(Na2S2O3)=0.1 mol/L] 4.7 Bromine Reference Titration Solution [c(1/2 Br2)=0.1 mol/L] 4.8 Potassium Bromate Reference Titration Solution [c(1/6 KBrO3)=0.1 mol/L] 4.9 Iodine Reference Titration Solution [c(1/2 I2)=0.1 mol/L] 4.10 Potassium Iodate Reference Titration Solution 4.11 Oxalic Acid (or Sodium Oxalate) Reference Titration Solution [c(1/2 H2C2O4)=0.1 mol/L or c(1/2 Na2C2O4)=0.1 mol/L] 4.12 Potassium Permanganate Reference Titration Solution [c(1/5 KMnO4)=0.1 mol/L] 4.13 Ammonium Iron (II) Sulfate Reference Titration Solution {c[(NH4)2Fe(SO4)2]=0.1 mol/L} 4.14 Cerium Sulphate (or Ammonium Cerium Sulfate) Reference Titration Solution {c[Ce(SO4)2]=0.1 mol/L or c[2(NH4)2SO4•Ce(SO4)2]=0.1 mol/L} 4.15 EDTA Reference Titration Solution 4.16 Zinc Chloride Reference Titration Solution 4.17 Magnesium Chloride (or Magnesium Sulfate) Reference Titration Solution [c(MgCl2)=0.1 mol/L or c(MgSO4)=0.1 mol/L] 4.18 Lead Nitrate Reference Titration Solution {c[Pb(NO3)2]=0.05 mol/L} 4.19 Sodium Chloride Reference Titration Solution [c(NaCl)=0.1 mol/L] 4.20 Sodium Thiocyanate (or Potassium Thiocyanate and Ammonium Thiocyanate) Reference Titration Solution [c(NaSCN)=0.1 mol/L, c(KSCN)=0.1 mol/L and c(NH4SCN)=0.1 mol/L] 4.21 Silver Nitrate Reference Titration Solution [c(AgNO3)=0.1 mol/L] 4.22 Mercuric Nitrate Reference Titration Solution 4.23 Sodium Nitrite Reference Titration Solution 4.24 Perchloric Acid Reference Titration Solution [c(HClO4)=0.1 mol/L] 4.25 Potassium Hydroxide-ethanol Reference Titration Solution [c(KOH)=0.1 mol/L] 4.26 Hydrochloric Acid - Ethanol Reference Titration Solution [c(HCl)=0.5 mol/L] 4.27 Ammonium Iron (III) Sulfate Reference Titration Solution {c[NH4Fe(SO4)2]=0.1 mol/L} Annex A (Normative) Correction Values of Reference Titration Solution Volume under Different Temperatures Annex B (Normative) Determination Method of Burette Capacity Annex C (Informative) Comparison Method of Partial Reference Titration Solutions Annex D (Informative) Expanded Uncertainty Evaluation of Reference Titration Solution Concentration Annex E (Informative) Processing Method of Mercury-contained Waste Liquid Annex F (Informative) Expanded Uncertainty Evaluation of Glass Container Capacity
Referred in GB/T 601-2016:
*GB/T 603-2002 Chemical Reagent – Preparations of Reagent Solution for Use in Tes
*GB/T 606-2003 Chemical reagent - General method for the determination of water - Karl Fischer method
*GB/T 6379.6-2009 Accuracy(trueness and precision) of measurement methods and results - Part 6: Use in practice of accuracy values
*GB/T 6682-2008 Water for analytical laboratory use - Specification and test methods
*GB/T 9725-2007 Chemical reagent—General rule for potentiometric titration
*JJG 130-2011 Verification Regulation of Liquid-in-Glass Thermometers for working
*JJG 196-2006 Verification Regulation of Working Glass Container
*JJG 1036-2008 Verification Regulation for Electronic Balance
GB/T 601-2016 is referred in:
* GB 8276-2006 Food additive - Glucoamylase preperation
*GB 10665-2004 Calcium carbide
*GB/T 15453-2008 Water for Industrial Circulating Cooling System and Boiler-Determination of Chloride
*GB 18582-2008 Indoor decorating and refurbishing materials - Limit of harmful substances of interior architectural coatings
*GB 18583-2008 Indoor decorating and refurbishing materials - Limit of harmful substances of adhesives
*QB/T 2317-2012 Oral care and cleansing products Calcium crude carbonate for Toothpaste
*GB/T 10288-2016 Testing methods for down and feather
*GB/T 20880-2007 Edible glucose
*QB/T 2968-2008 Determination of strontium chloridein in toothpastes
*QB/T 2477-2007 Dicalcium phosphate dihydrate for toothpaste
*GB/T 1576-2008 Water quality for industrial boilers
*GB/T 605-2006 Chemical reagent - General method for the measurement of colour
*GB 1987-2007 Food additive—Ctric acid
*FZ/T 50014-2008 Method for the determination of residual sulphur in viscoce fibres-direct iodimetry
*GB/T 18952-2017 Rubber compounding ingredients―Sulfur and methods of test
*GB/T 8372-2017 Toothpaste
*GB 8851-2005 Food additive Propyl p-hydroxybenzoate
*GB/T 3185-2016 Zinc oxide ( Indirect method)
*GB/T 25865-2010 Feed additive—Zinc sulphate
*NY/T 2118-2012 Plug seedling substrate of vegetables
*GB/T 14235.1-2018 Low temperature pattern wax material for investment casting—Part 1:Testing methods for physical properties
*SH/T 1817-2017 Plastics. Determination of residual acetaldehyde in polyethylene terephthalate(PET)resin for bottles. Headspace gas chromatography
*GB/T 2093-2011 Formic acid for industrial use
*HG/T 4873-2016 Ethylene glycol monomethyl ether for industrial use
*GB/T 20708-2019 Limit and determination of parts of harmful substances in textile dyeing and finishing auxiliaries
*GB/T 639-2008 Chemical reagent - Sodium carbonate anhydrous
*GB/T 17810-2009 Feed grade DL-methionine
*GB/T 23973-2018 Determination of formaldehyde in dye products
*GB 22549-2017 Feed additive - Dicalcium phosphate
*GB/T 21996-2008 Feed additive—Ferric glycine complex
*GB 35373-2017 HFC fire extinguishing agents
*GB 15892-2020 Polyaluminium chloride for treatment of drinking water
*QB/T 2966-2014 Functional Toothpastes
*HG/T 2542-2014 Trichloroethylene for industrial use
*FZ/T 50018-2013 Determination of the protein content of the protein viscose fiber
*GB/T 24695-2009 Cellophane used for food packaging
*GB/T 4117-2008 Methylene chloride for industrial use
*GB 19106-2013 Sodium hypochlorite
*HG/T 2471-2011 Coating of dimensionally stable anode for electrolyzer
*HG/T 3679-2011 Ruthenium trichloride for dimensionally stable anode coating in electrolyzer
*QB/T 2945-2012 Oral rinses
*GB/T 209-2018 Sodium hydroxide for industrial use
*GB/T 12589-2007 Chemical reagent—Ethyl acetate
*GB/T 6026-2013 Acetone for Industrial Use
*GB/T 1287-1994 Chemical reagent. Nickel sulfate hexahydrate
*GB/T 15355-2008 Chemical reagent - Nickel chloride hexahydrate
*GB/T 9853-2008 Chemical reagent - Sodium sulfate anhydrous
*GB/T 646-2011 Chemical reagent—Potassium chloride
*SY/T 6280-2006 Health safety and environment management specification for seismic crew
*GB/T 6820-2016 Ethanol for industrial use
*GB/T 626-2006 Chemical reagent - Nitric acid
*GB/T 534-2014 Sulphuric acid for industrial use
*HG/T 3473-2003 Chemical reagent Iron powder reduced
*GB/T 1266-2006 Chemical reagent - Sodium chloride
*QB/T 4857-2015 Tooth strips
*GB/T 33107-2016 Dimethyl carbonate for industrial use
*DL/T 1705-2017 Phosphate ester fire-resistant-determination of ageing-closed cup amethod
*GB/T 20882.2-2021 Quality requirements for starch sugar—Part 2: Glucose syrup and glucose syrup powder
*GB/T 394.2-2008 General methods of analysis for ethanol
*GB 15892-2009 Poly aluminium chloride for treatment of drinking water
*GB/T 1677-2008 Determinating the epoxy value of plasticizers
*GB/T 14684-2022 Sand for construction
*GB/T 22114-2021 Humectants for toothpastes - Glycerin and polyethylene glycol
*HG/T 2089-2014 Test method of activity for oxidizing sulphuric dioxide into sulphuric acid catalyst
*GB/T 32461-2015 Determination of formaldehyde in amino resins and phenolic resins and of migration of formaldehyde in their moldings―High performance liquid chromatography
*GB/T 20886.2-2021 Quality requirements for yeast products—Part 2: Processed yeast products
*GB 20371-2016 Soy protein for food industry
*GB/T 20886.1-2021 Quality requirements for yeast products—Part 1:Yeast for food processing
*GB/T 14233.1-2022 Test methods for infusion,transfusion,injection equipments for medical use―Part 1:Chemical analysis methods
*GB/T 12009.2-2016 Plastics―Aromatic isocyanates for use in the production of polyurethane―Part 2:Determination of hydrolysable chlorine
Code of China
Standard
GB/T 601-2016  Chemical Reagent - Preparations of Standard Volumetric Solutions (English Version)
Standard No.GB/T 601-2016
Statusvalid
LanguageEnglish
File FormatPDF
Word Count22500 words
Price(USD)280.0
Implemented on2017-5-1
Deliveryvia email in 1 business day
Detail of GB/T 601-2016
Standard No.
GB/T 601-2016
English Name
Chemical Reagent - Preparations of Standard Volumetric Solutions
Chinese Name
化学试剂 标准滴定溶液的制备
Chinese Classification
Professional Classification
GB
ICS Classification
Issued by
AQSIQ,SAC
Issued on
2016-10-13
Implemented on
2017-5-1
Status
valid
Superseded by
Superseded on
Abolished on
Superseding
GB/T 601-2002 Chemical Reagent - Preparations of Standard Volumetric Solutions
Language
English
File Format
PDF
Word Count
22500 words
Price(USD)
280.0
Keywords
GB/T 601-2016, GB 601-2016, GBT 601-2016, GB/T601-2016, GB/T 601, GB/T601, GB601-2016, GB 601, GB601, GBT601-2016, GBT 601, GBT601
Introduction of GB/T 601-2016
1 Scope This standard specifies preparation and calibration method of chemical reagent reference titration solution. This standard is applicable to both preparation and calibration of reference titration solution whose chemical reagent purity and impurity content is determined by titration and other areas. 2 Normative References The following documents for the application of this document are essential. For dated reference, only the edition cited applies. For undated references, the latest edition (including any amendments) applies. GB/T 603 Chemical Reagent - Preparations of Reagent Solutions for Use in Test Method GB/T 606 Chemical Reagent - General Method for the Determination of Water - Karl Fischer Method GB/T 6379.6-2009 Accuracy(trueness and precision) of Measurement Methods and Results - Part 6: Use in Practice of Accuracy Values GB/T 6682 Water for Analytical Laboratory Use-Specification and Test Methods GB/T 9725-2007 Chemical Reagent - General Rule for Potentiometric Titration JJG 130 Verification Regulation of Liquid-in-Glass Thermometers for Working JJG 196-2006 Verification Regulation of Working Glass Container JJG 1036 Verification Regulation for Electronic Balance 3 General Requirements 3.1 Unless otherwise specified in this standard, the analytically pure level and above reagents, preparations and products prepared according to GB/T 603 and Grade 3 water (defined in GB/T 6682) shall be adopted for the purpose of this standard. 3.2 The concentration of reference titration solution prepared in this standard refers to that at 20℃ except perchloric acid reference titration solution, hydrochloric acid-ethanol reference titration solution and sodium nitrite reference titration solution [c(NaNO2)=0.5 mol/L]. If calibration, direct preparation and use of reference titration solution is not conducted at 20℃, volume of shall be corrected (see Annex A). Reference titration solution with "calibration prior to use" may not be corrected in case of not large temperature difference during calibration and use. Calibration, direct preparation and analytical balance, burette, one-mark volumetric flask and one-mark pipet for use shall be verified or calibrated periodically according to relevant verification regulation and determination method of burette volume is performed according to Annex B. Besides, one-mark volumetric flask and one-mark pipet shall be provided with volume correction factor.
Contents of GB/T 601-2016
Foreword i 1 Scope 2 Normative References 3 General Requirements 4 Preparation and Calibration of Reference Titration Solution 4.1 Sodium Hydroxide Reference Titration Solution 4.2 Hydrochloric Acid Reference Titration Solution 4.3 Sulfuric Acid Reference Titration Solution 4.4 Sodium Carbonate Reference Titration Solution 4.5 Potassium Bichromate Reference Titration Solution [c(1/6 K2Cr2O7)=0.1 mol/L] 4.6 Sodium Thiosulfate Reference Titration Solution [c(Na2S2O3)=0.1 mol/L] 4.7 Bromine Reference Titration Solution [c(1/2 Br2)=0.1 mol/L] 4.8 Potassium Bromate Reference Titration Solution [c(1/6 KBrO3)=0.1 mol/L] 4.9 Iodine Reference Titration Solution [c(1/2 I2)=0.1 mol/L] 4.10 Potassium Iodate Reference Titration Solution 4.11 Oxalic Acid (or Sodium Oxalate) Reference Titration Solution [c(1/2 H2C2O4)=0.1 mol/L or c(1/2 Na2C2O4)=0.1 mol/L] 4.12 Potassium Permanganate Reference Titration Solution [c(1/5 KMnO4)=0.1 mol/L] 4.13 Ammonium Iron (II) Sulfate Reference Titration Solution {c[(NH4)2Fe(SO4)2]=0.1 mol/L} 4.14 Cerium Sulphate (or Ammonium Cerium Sulfate) Reference Titration Solution {c[Ce(SO4)2]=0.1 mol/L or c[2(NH4)2SO4•Ce(SO4)2]=0.1 mol/L} 4.15 EDTA Reference Titration Solution 4.16 Zinc Chloride Reference Titration Solution 4.17 Magnesium Chloride (or Magnesium Sulfate) Reference Titration Solution [c(MgCl2)=0.1 mol/L or c(MgSO4)=0.1 mol/L] 4.18 Lead Nitrate Reference Titration Solution {c[Pb(NO3)2]=0.05 mol/L} 4.19 Sodium Chloride Reference Titration Solution [c(NaCl)=0.1 mol/L] 4.20 Sodium Thiocyanate (or Potassium Thiocyanate and Ammonium Thiocyanate) Reference Titration Solution [c(NaSCN)=0.1 mol/L, c(KSCN)=0.1 mol/L and c(NH4SCN)=0.1 mol/L] 4.21 Silver Nitrate Reference Titration Solution [c(AgNO3)=0.1 mol/L] 4.22 Mercuric Nitrate Reference Titration Solution 4.23 Sodium Nitrite Reference Titration Solution 4.24 Perchloric Acid Reference Titration Solution [c(HClO4)=0.1 mol/L] 4.25 Potassium Hydroxide-ethanol Reference Titration Solution [c(KOH)=0.1 mol/L] 4.26 Hydrochloric Acid - Ethanol Reference Titration Solution [c(HCl)=0.5 mol/L] 4.27 Ammonium Iron (III) Sulfate Reference Titration Solution {c[NH4Fe(SO4)2]=0.1 mol/L} Annex A (Normative) Correction Values of Reference Titration Solution Volume under Different Temperatures Annex B (Normative) Determination Method of Burette Capacity Annex C (Informative) Comparison Method of Partial Reference Titration Solutions Annex D (Informative) Expanded Uncertainty Evaluation of Reference Titration Solution Concentration Annex E (Informative) Processing Method of Mercury-contained Waste Liquid Annex F (Informative) Expanded Uncertainty Evaluation of Glass Container Capacity
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Keywords:
GB/T 601-2016, GB 601-2016, GBT 601-2016, GB/T601-2016, GB/T 601, GB/T601, GB601-2016, GB 601, GB601, GBT601-2016, GBT 601, GBT601